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Batch Distillation in Chemical & Process Engineering
Introduction
Welcome to the Course (1:17)
Content Index (4:24)
Mass Transfer Review
2 Reveiw - Mass Transfer. (0:59)
Ideal Gas Law (3:43)
Ideal Solution (5:02)
Vapor Pressure (5:29)
Partial Pressure (3:44)
Partial Pressure vs Vapor Pressure (3:42)
Task Pressures (0:38)
What is Vapor Liquid Equilibrium for Pure substances (4:36)
Vapor Liquid Equilibrium for Binary Systems (6:55)
2.2 Volatility (Chemistry) (4:25)
Task - Volatility of Substances (1:36)
2.3 Binary Diagrams (1:45)
Bubble Point (3:03)
Case 1 - Ideal solution and Ideal Gas (2:02)
Henry's Law (2:21)
Ex - Raoults Law Application (9:09)
Dew Point (2:38)
Case 4 - Real Solution - Real Gases (3:17)
Introduction to Azeotropic Distillation (2:20)
Getting VLE Data from NIST Databases (3:13)
K-Values - An Overview (2:27)
T-XY Diagram (3:26)
Cases in Vapor-Liquid Equilibrium (2:43)
Ex - Henrys Law for Solubility (6:29)
P-XY Diagrams (5:16)
K-Values (revisited) (2:55)
Task - Reading P-XY Diagrams (2:22)
Task - XY Diagram (2:21)
Task - Extracting Binary Data using NIST Database (3:27)
Task - Reading T-XY Diagram (0:41)
Maximum Boiling Azeotrope (2:29)
Task - Identify Azeotrope Types (1:26)
What is Aspen Plus (1:31)
Case 3 - Ideal Solution and Real Gas (2:36)
Case 2 - Real Soltion - Ideal Gas (3:33)
Azeotropes (3:40)
Relative Volatility (8:06)
Special Case - Constant Relative Volatility (2:37)
Miniumum boiling Azeotropes (4:04)
Task - Prove Phase Rule for VLE systems (2:18)
Task - Calculate K-Values (4:01)
Cases Conclusions - Ideal Gases and Solutions vs Real Gases and Solutions (1:58)
Phase Rules & Diagrams (11:05)
Analysis of T-XY Diagram (5:31)
Non-Ideal Solutions (4:49)
XY Diagrams (3:41)
2.5 Devitations (4:49)
Raoult's Law (6:30)
2.6 Getting VLE Data from Aspen Plus (2:41)
Batch Distillation Overview
What is Batch Distillation (9:01)
The Key Concept - Time (4:47)
Animation - Batch Distillation (5:47)
Task - Batch Distillation Column Control Lab (0:42)
4.2 Introduction to Batch Distillation (2:41)
Advantages of Batch Distillation (6:18)
General Disadvantages of the BAtch Distillation (3:02)
Batch Distillation - Operation and Control of Loads (4:25)
Reflux Control in Batch Distillation (Operation and Control) (6:00)
Batch Distillation with Rectifying Sections (6:41)
Simple Batch Distillation
4.1 Introduction to Simple Differential Distillation (13:12)
The Rayleigh Equation for Simple Fractional Distillation (8:42)
Analytical & Graphical Solutions for Rayleigh Equation in Batch Distillation (6:35)
Ex. 1 Application of Rayleigh Equation to Isopropanol Water Mix (9:38)
Ex.2 Partial Rayleigh Distillation of Hexane and JHeptane (18:29)
Ex.3 Rayleigh Equation using Equilbirium Expresion in Distillation (10:34)
Ex. 4 Distillation using Rayleigh Equation given time conditions (7:23)
Advanced Batch Distillation
Equilbirium Stages Overview in Batch Distillation (10:37)
An Overview of McCabe Thiele Method in Batch Distillation (8:20)
Operation Line of a Batch Distillation (Rectifiers) (13:45)
Batch Distillation operating at Constant Reflux (8:30)
Derivation of the Batch Distillation for Constant Reflux (4:18)
Task - Proof of Raliegh Equation form the Batch Distillation Equation (0:42)
Graphical Method using a Batch Distillator with Constant Reflux (3:12)
Constant Composition Case for Batch Distillation (13:46)
Closure
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Ex. 1 Application of Rayleigh Equation to Isopropanol Water Mix
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